Derivatization in Mass Spectrometry—1. Silylation (Q30930859)

27 June 2017

1 reference

title

Derivatization in mass spectrometry--1. Silylation (English)

1 reference

27 June 2017

Derivatization in Mass Spectrometry—1. Silylation (English)

1 reference

2 January 2024

author name string

John M. Halket

1

1 reference

https://www.ebi.ac.uk/europepmc/webservices/rest/search?resulttype=core&format=json&query=SRC%3AMED%20AND%20EXT_ID%3A12748398

reference URL

2 January 2024

Vladimir G. Zaikin

2

1 reference

https://www.ebi.ac.uk/europepmc/webservices/rest/search?resulttype=core&format=json&query=SRC%3AMED%20AND%20EXT_ID%3A12748398

reference URL

2 January 2024

language of work or name

English

1 reference

National Center for Biotechnology Information

https://eutils.ncbi.nlm.nih.gov/entrez/eutils/esummary.fcgi?db=pubmed&retmode=json&id=12748398

reference URL

2 January 2024

publication date

1 January 2003

1 reference

full work available at URL

27 June 2017

http://journals.sagepub.com/doi/pdf/10.1255/ejms.527

1 reference

European Journal of Mass Spectrometry

2 January 2024

published in

1 reference

27 June 2017

volume

9

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27 June 2017

issue

1

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27 June 2017

page(s)

1-21

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Derivatization procedures for gas chromatographic-mass spectrometric determination of xenobiotics in biological samples, with special attention to drugs of abuse and doping agents.

27 June 2017

cites work

2

1 reference

Comprehensive screening procedure for detection of stimulants, narcotics, adrenergic drugs, and their metabolites in human urine

2 January 2024

3

1 reference

Determination of fatty acid amides as trimethylsilyl derivatives by gas chromatography with mass spectrometric detection

2 January 2024

17

1 reference

Trimethylsilylation of amino acids derivatization and chromatography

2 January 2024

18

1 reference

Analysis of amino acids as their tert.-butyldimethylsilyl derivatives by gas-liquid chromatography and mass spectrometry

2 January 2024

19

1 reference

Gas chromatography-mass spectrometry of trimethylsilyl derivatives of omega-amino acids

2 January 2024

20

1 reference

2 January 2024

24

15

55

Osthoff R.C.

1957

1 reference

Derivatives of the Methylchlorosilanes. I. Trimethylsilanol and its Simple Ethers

2 January 2024

25

1 reference

A new silylation reagent for amino acids bis (trimethylsilyl)trifluoroacetamide (BSTFA)

2 January 2024

26

1 reference

The use of different silylating agents for structure analyses of steroids

2 January 2024

31

1 reference

Examination of the diphenylpropanoids of nutmeg as their trimethylsilyl, triethylsilyl and tri-n-propylsilyl derivatives using combined gas chromatography and mass spectrometry

2 January 2024

33

1 reference

Use of new silylating agents for identification of hydroxylated steroids by gas chromatography and gas chromatography mass spectrometry

2 January 2024

35

1 reference

Specific reduction of E prostaglandins to F.alpha. prostaglandins and prostaglandin E2 to prostaglandin E1

2 January 2024

36

1 reference

Protection of hydroxyl groups as tert-butyldimethylsilyl derivatives

2 January 2024

37

1 reference

Evaluation of allyldimethylsilyl ethers as steroid derivatives for gas chromatography-mass spectrometry

2 January 2024

38

1 reference

Dimethyldiacetoxy silane as a silylating reagent. A new technique for forming siliconides of corticosteroids

2 January 2024

48

1 reference

Use of silylating agents for the identification of hydroxylated steroids by gas chromatography and gas chromatography-mass spectrometry. Discrimination between phenolic and alcoholic hydroxyl groups

2 January 2024

51

1 reference

Artifacts in trimethylsilyl derivatization reactions and ways to avoid them

2 January 2024

54

1 reference

Use of t-butyldimethylchlorosilane/imidazole reagent for identification of molecular species of phospholipids by gas-liquid chromatography mass spectrometry

2 January 2024

65

1 reference

Femtomole level of analysis of biogenic amines and amino acids using functional group mass spectrometry

2 January 2024

66

1 reference

Derivatization procedures for the detection of beta(2)-agonists by gas chromatographic/mass spectrometric analysis

2 January 2024

69

1 reference

Analysis of anabolic steroids using GC/MS with selected ion monitoring.

2 January 2024

71

1 reference

Diagnostic fragmentation of saturated and unsaturated fatty acids by gas chromatography-mass spectrometry with pentafluorophenyldimethylsilyl derivatization

2 January 2024

73

1 reference

Identification of fatty acid amides in human plasma

2 January 2024

74

1 reference

Investigation of group migration in the fragmentation of bis(trimethylsilyl) ethers of diols separated by rigid groups

2 January 2024

76

1 reference

Trimethylsilyl group migration during electron impact and chemical ionization mass spectrometry of the trimethylsilyl ethers of 20-hydroxy-5alpha-pregnan-3-ones and 20-hydroxy-4-pregnen-3-ones

2 January 2024

77

1 reference

Quantitative analysis of gas-phase formaldehyde molecular species at equilibrium with formalin solution

2 January 2024

81

1 reference

Determination of testosterone:epitestosterone ratio after pentafluorophenyldimethylsilyl-trimethylsilyl derivatisation using gas chromatography-mass spectrometry in equine urine

2 January 2024

84

1 reference

GC-MS determination of steroids related to androgen biosynthesis in human hair with pentafluorophenyldimethylsilyl-trimethylsilyl derivatisation

2 January 2024

85

1 reference

Automated screening of urine samples for carbohydrates, organic and amino acids after treatment with urease

2 January 2024

86

1 reference

Diagnosis of inborn errors of metabolism using filter paper urine, urease treatment, isotope dilution and gas chromatography-mass spectrometry.

2 January 2024

87

1 reference

Deconvolution gas chromatography/mass spectrometry of urinary organic acids--potential for pattern recognition and automated identification of metabolic disorders

2 January 2024

88

1 reference

Identification by combined gas chromatography-mass spectrometry of constituent long-chain fatty acids and alcohols from the meibomian glands of the rat and a comparison with human meibomian lipids

2 January 2024

89

1 reference

Long-chain fatty acids and alcohols from gerbil meibomian lipids

2 January 2024

90

1 reference

Silyl derivatization of alkylphenols, chlorophenols, and bisphenol A for simultaneous GC/MS determination

2 January 2024

92

1 reference

A multiresidue derivatization gas chromatographic assay for fifteen phenolic constituents with mass selective detection

2 January 2024

93

1 reference

Gas chromatographic-mass spectrometric determination of plasma saturated fatty acids using pentafluorophenyldimethylsilyl derivatization

2 January 2024

94

1 reference

Gas-liquid chromatography-mass spectrometry of mono- and dithiols as their tert.-butyldimethylsilyl derivatives

2 January 2024

98

1 reference

Capillary gas chromatography of amino acids, including asparagine and glutamine: sensitive gas chromatographic-mass spectrometric and selected ion monitoring gas chromatographic-mass spectrometric detection of the N,O(S)-tert.-butyldimethylsilyl der

2 January 2024

100

1 reference

Use of ion trap gas chromatography-tandem mass spectrometry for detection and confirmation of anabolic substances at trace levels in doping analysis

2 January 2024

101

1 reference

ESI mass spectrometry of amino acid trimethylsilylethyl esters.

2 January 2024

104

1 reference

2 January 2024

Identifiers

DOI

10.1255/EJMS.527

0 references

1 reference